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Make Anhydrous Ferrous Chloride

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Apr 30, 2016
5:43

Glassware generously provided by http://www.alchemylabsupply.com/ Use the discount code "copper" for a 5% discount. Donate to NurdRage! Through Patreon (preferred): https://www.patreon.com/NurdRage Through Bitcoin: 1NurdRAge7PNR4ULrbrpcYvc9RC4LDp9pS Videos referenced in this video: Make chlorotoluene: https://www.youtube.com/watch?v=khfYvY_Gczk Make ferric chloride (hydrated): https://www.youtube.com/watch?v=43Xsh9J7S-g In this video we make ferrous chloride. First we react 57g of iron metal with 200mL of 30% hydrochloric acid and 300mL of methanol. Once hydrogen evolution ceases the mixture is filtered. One or two large iron nails are placed in the flask and an air-tight simple distillation is assembled. The exhaust port on the distillation adapter is connected to a vacuum system and the distillation is performed under reduced pressure. Once the ferrous chloride is dried, the flask is stoppered and stored until needed. This video was generously sponsored by: Robert Boll Kevin S Only HR Scott Malcheski advisable Michael Zappe Emil Mikulic Dino Capiaghi Benjamin Nied Wesley Gardner LVE Meshal Al-Enazi Lord Martin Hill Matthew Brunette Collin Wright Simon Bitdiddle Cullen Purkis Samuel Pelzer Carl Potter Max Loutzenheiser Jack kelly Phillip Hutchings

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Make Anhydrous Ferrous Chloride | NatokHD